Peer-reviewed literature directly characterizes copper as a diamagnetic material and reports negative magnetic susceptibility measurements consistent with this classification.
Even though microcoils improve the sensitivity of NMR measurement of tiny samples, magnetic-field inhomogeneity due to the bulk susceptibility effect of the coil material can cause serious resonance-line broadening. Here, we propose to fabricate the microcoil using a thin, hollow copper capillary instead of a wire and fill paramagnetic liquid inside the capillary, so as to cancel the diamagnetic contribution of the copper. Susceptibility cancellation is demonstrated using aqueous solution of NiSO4. In addition, the paramagnetic liquid serves as coolant when it is circulated through the copper capillary, effectively transferring the heat generated by radiofrequency pulses.
The ball end magnetorheological finishing (BEMRF) is an advanced nanofinishing process for flat, curved and freeform surfaces of ferromagnetic as well as diamagnetic materials. While finishing copper (diamagnetic material) by this process, a low finishing effect is obtained as its surface repels the externally applied magnetic field. In this work a magnetic simulation is carried out over both copper and ferromagnetic material. For the ferromagnetic material the simulation result shows a high flux density region below the tool tip. However in case of copper the magnetic flux density is too low for finishing. It is also observed through simulations that when copper workpiece is placed on a mild steel base the flux density improves marginally. This led to the idea of using a permanent magnet (in place of mild steel) as a base for finishing of copper using the BEMRF process. Using this technique copper was finished and the experimental results indicate that this method can realize ultra-precision finishing of copper.
We report on a method of measuring the high-field susceptibilities of paramagnetic and diamagnetic materials using only a standard NMR system equipped with pulsed field gradients. We demonstrate the accuracy and sensitivity of the technique by measuring a series of 99.9% copper wires with diameters between 0.16 mm and 0.79 mm. We measured the volumetric susceptibility of the copper to be χ=-9.5±0.2·10(-6), which agrees with the literature value of pure copper, -9.6·10(-6). In addition to making quantitative measurements, this technique can also be used to evaluate the effectiveness of compensation schemes used to produce "zero-susceptibility" materials needed for construction of high-resolution NMR probes.
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